By R. Stuart Tipson and Derek Horton (Eds.)
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Extra resources for Advances in Carbohydrate Chemistry and Biochemistry 47
E. B u g , in B. Pullman and N. ),Metal-Ligandlnteractions in Organic Chemistry and Biochemistry, Part 2, Reidel Publishing Company, Dordrecht (Holland), 1977, pp. 231 -256. (77) C. A. Beevers and W. Cochran, Proc. R. London, Ser. A, 190 (1947) 257-272. (78) D. C. Craig, N. C. Stephenson, and J. D. , 22 (1972) 494-495. (79) D. J. Wilbur, C. Williams, and A. Allerhand, J. Am. Chem. , 99 (1977) 5450-5452. s1)In this adduct, the calcium ion is coordinated to 0-1,O-2, and 0-3 of one D-mannose molecule, to 0-5 and 0-6 of another one, and to three water molecules; the resulting, eight-fold coordination is the most common one for calcium ions in carbohydrate adduckS2The cation is slightly closer to the water molecules than to the hydroxyl groups (this is generally true for sugar -calcium chloride adductss2)and slightlycloser to 0-2 than to 0-1 and 0-3; but none of these distances differs much from the average (244 pm).
There is also the question of the stoichiometry of the complexes. 23Most authors have . 94 Despite these difficulties, approximate “stability constants,” calculated for 1 : 1 complexes, are useful, because they allow comparison of the complexing ability of various cations and various polyols, and they enable the calculation of the approximate extent of complex-formation at different concentrations. Two methods have been mainly used for the determination of the stability constants of cation - sugar complexes.
V. Bilik, D. Anderle, and J. Alfoldi, Chem. Zvesti, 28 (1974) 668-672. J. Defaye, A. Gadelle, and S. J. Angyal, Carbohydr. , 126 (1984) 165- 169. J. R. Rasmussen, S. R. Tafuri, and S . T. Smale, Carbohydr. , 1 16 (1983) 2 1-29. L. Hough and E. OBrien, Carbohydr. , 84 (1980) 95- 102. M. K. Das, D. G. Streefkerk, and C. P. J. Glaudemans, Mol. , 16 (1979) 97- 100. S. J. Angyal, C. L. Bodkin, J. A. Mills, and P. M. Pojer, Aust. J. , 30 (1977) 1259-1268. S. J. Angyal, C. L. Bodkin, and F. W. Parrish, Aust.
Advances in Carbohydrate Chemistry and Biochemistry 47 by R. Stuart Tipson and Derek Horton (Eds.)
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